HS-SPME-GC-MS分析川芎茶调制剂不同剂型的挥发性成分  

Analysis of volatile components in different dosage forms of Chuanxiong Chatiao preparations by HS-SPME-GC-MS

作　　者：王文通 江汉美[1] 甘剑锋 WANG Wen-tong;JIANG Han-mei;GAN Jian-feng(Hubei University of Chinese Medicine/Research and Development Center of Medicinal Plant in Hubei Province,Wuhan 430065,China)

机构地区：[1]湖北中医药大学/湖北省药用植物研发中心,武汉430065

出　　处：《湖北农业科学》2020年第11期112-119,共8页Hubei Agricultural Sciences

基　　金：湖北省技术创新专项重大项目(2016ACA146)。

摘　　要：采用顶空固相微萃取(HS-SPME)与气质联用法(GC-MS)对川芎茶调制剂不同剂型的挥发性成分进行比较。结果表明,在川芎茶调颗粒中共分离出24个峰,鉴定出16种成分,占其总挥发性成分的89.13%;在川芎茶调片中分离出63个峰,鉴定出46种成分,占其总挥发性成分的80.91%;在川芎茶调丸(浓缩丸)中分离出94个峰,鉴定出69种成分,占其总挥发性成分的90.10%;在川芎茶调丸(水丸)中分离出101个峰,鉴定出68种成分,占其总挥发性成分的78.50%。川芎茶调制剂的不同剂型的挥发性成分和相对百分含量存在一定的差异。HS-SPME-GC-MS was used for analysis the volatile components of Chuanxiong Chatiao preparations in different dosage forms.The results showed that 16 components were identified in the 24 peaks separated by Chuanxiong Chatiao granule,which ac⁃counted for 89.13%of the total volatile components.46 components were identified in the 63 peaks separated by Chuanxiong Chatiao tablet,which accounted for 80.91%of the total volatile components.69 components were identified in the 94 peaks separated by Ch⁃uanxiong Chatiao pill(concentrated pills),which accounted for 90.10%of the total volatile components.68 components were identi⁃fied in the 101 peaks separated by Chuanxiong Chatiao pill(water-bindered pills),which accounted for 78.50%of the total volatile components.The volatile components in different dosage forms of Chuanxiong Chatiao Preparations were different in chemical composi⁃tions and content.

关 键 词：川芎茶调制剂 剂型 HS-SPME-GC-MS 挥发性成分 

分 类 号：O657.7[理学—分析化学]