基于近红外漫反射光谱的面包老化过程中非冻结水含量无损检测  

Non-destructive detection of non-frozen water content during bread aging based on near infrared diffuse reflection spectroscopy

作　　者：闫奕霏 高薪 汤修映[1] YAN Yi-Fei;GAO Xin;TANG Xiu-Ying(College of Engineering,China Agricultural University,Beijing 100083,China)

机构地区：[1]中国农业大学工学院,北京100083

出　　处：《食品安全质量检测学报》2022年第22期7264-7271,共8页Journal of Food Safety and Quality

基　　金：国家重点研发计划项目(2019YFC1605303)。

摘　　要：目的建立一种基于近红外光谱技术快速无损测定面包老化过程中的非冻结水含量的方法。方法应用近红外漫反射光谱技术采集新鲜面包在放置2 h、2 d、3 d、4 d、5 d、6 d、7 d时的光谱,对比导数、卷积平滑(Savitzky-Golay,S-G)、标准正态变量变换(standard normal variable transformation,SNV)及多元散射校正(multiplicative scatter correction,MSC)预处理方法,利用偏最小二乘回归法(partial least square regression,PLSR)和多元线性回归法(multiple linear regression,MLR)建立面包老化过程中的非冻结水含量的预测模型,并对比两种模型预测结果。结果利用PLSR建模相较MLR建模结果较好,建立的模型预测结果较好,模型的校正集相关系数和均方根误差分别为0.9386和0.0236,验证集相关系数和均方根误差分别为0.9271和0.0245。结论通过近红外光谱技术结合PLSR法建立面包老化过程中的非冻结水含量模型可作为面包老化过程中的非冻结水含量无损快速测定的可行性方法,其含量变化可以有效预测面包老化,为面包老化的无损检测提供了新的可行方案。Objective To establish a rapid and non-destructive method for the determination of non-frozen water content in bread aging process based on near infrared spectroscopy.Methods Near infrared diffuse reflectance spectroscopy was used to collect the spectra of fresh bread at 2 h,2 d,3 d,4 d,5 d,6 d and 7 d,and the pretreatment methods of derivative,Savitzky-Golay smooth(S-G),standard normal variable transformation(SNV)and multiple scatter correction(MSC)were compared,partial least square regression(PLSR)and multiple linear regression(MLR)were used to establish the prediction model of non frozen water content during bread aging,and the prediction results of the two models were compared.Results The results of PLSR modeling were better than those of MLR modeling,and the prediction results of the established model were better.The correlation coefficient and root mean square error of the model were 0.9386 and 0.0236 respectively,and the correlation coefficient and root mean square error of the validation set were 0.9271 and 0.0245,respectively.Conclusion The model of non-frozen water content in bread aging process established by near infrared spectroscopy combined with PLSR method can be used as a feasible method for nondestructive and rapid determination of non-frozen water content in bread aging process.The change of its content can effectively predict the aging of bread,and provide a new feasible scheme for nondestructive testing of bread aging.

关 键 词：面包老化 非冻结水 近红外光谱 偏最小二乘回归法 

分 类 号：TS213.21[轻工技术与工程—粮食、油脂及植物蛋白工程] O657.33[轻工技术与工程—食品科学与工程]