无机化学实验教学融入前沿科研成果初探——以TiC负载Ir的合成及其在电解水中的应用为例  

Integrating Frontier Scientific Research Achievements into Undergraduate Teaching of Inorganic Synthetic Chemistry Experiment:A Case Study of the Synthesis of Ir/TiC and Its Application in Oxygen Evolution

作　　者：章本天 张婷 柏雷 姚湾湾 叶龙强 李子荣 Zhang Bentian;Zhang Ting;Bai Lei;Yao Wanwan;Ye Longqiang;Li Zirong(College of Chemistry and Materials Engineering,Anhui Science and Technology University,Bengbu 233000,China)

机构地区：[1]安徽科技学院化学与材料工程学院,安徽蚌埠233000

出　　处：《广东化工》2024年第15期179-181,共3页Guangdong Chemical Industry

基　　金：教育部产学合作协同育人项目(230804429241319,220605940245812);应用化学专业改造提升项目(2023zygzts055);安徽省“六卓越一拔尖”项目(2022zybj026);安徽科技学院审核性评估专项(X2021072)。

摘　　要：无机化学实验是培养应用化学专业本科生发散性思维和辩证唯物主义世界观的关键训练环节之一,鉴于纳米无机材料在新能源领域的广泛应用,结合本科生学习特点,本文以典型的无机材料合成教学内容为例,首先设计碳热还原法和液相还原法合成Ir/TiC催化剂,通过X射线粉末衍射仪、透射电镜仪器对催化剂晶型和形貌进行表征分析,之后应用电化学工作站和电解槽系统评价了催化剂的性能。设计成综合化学实验教学,不仅增强学生无机材料制备分析能力的同时,而且助力学生与科学前沿研究成果“接轨”,提升科学素养。The experiment of inorganic chemistry is one of the key training links for undergraduates mastering the theoretical knowledge of inorganic chemistry,which can cultivate students'divergent thinking and dialectical materialism world view through experimentation.In view of the wide application of nano-inorganic materials in the field of new energy,a typical inorganic material synthesis teaching content is taken as an example to design a carbon-thermal reduction method and liquid phase reduction method to synthesize TiC materials,and as a carrier supported Ir in the electrocatalytic oxygen evolution reaction application.The crystal shape and morphology of the catalyst were characterized by X-ray powder diffractometer and transmission electron microscopy,and then the performance of the catalyst was evaluated by electrochemical workstation and electrolyzer.This experiment plays a significant role in exercising students'ability to prepare inorganic materials,understanding the scientific frontier,and improving scientific literacy.

关 键 词：本科实验教学 无机化学 TiC纳米材料 析氧反应 前沿科学 

分 类 号：G64[文化科学—高等教育学] O6[文化科学—教育学]