综合教学实验设计:Co(OH)_(2)衍生的S,N-CoMOF催化剂制备及其电氧化性能研究  

Comprehensive Teaching Experiment Design:Preparation and Electrooxidation Performance of S,N-CoMOF Catalysts Derived from Co(OH)_(2)

作　　者：刘艳艳[1] 程燚 叶舒杭 林伟伟 柴俊 LIU Yanyan;CHENG Yi;YE Shuhang;LIN Weiwei;CHAI Jun(College of Chemical and Environmental Engineering,Anhui Polytechnic University,Anhui Wuhu 241000;The High School Affiliated to Anhui Normal University,Anhui Wuhu 241000,China)

机构地区：[1]安徽工程大学化学与环境工程学院,安徽芜湖241000 [2]安徽师范大学附属中学,安徽芜湖241000

出　　处：《广州化工》2025年第5期198-201,208,共5页GuangZhou Chemical Industry

基　　金：安徽工程大学大学生创新创业训练计划项目(No:202310363280);安徽工程大学课程思政优质课(No:2022szyzk67)。

摘　　要：设计介绍了一个综合电化学实验——采用简单的水热反应和化学浸泡两步制备了S,N-CoMOF/CC电催化剂,通过对其催化剂形貌结构、物相组成的表征及电催化5-羟甲基糠醛(HMF)氧化性能的测试,使得学生初步掌握无机纳米复合材料的制备过程、表征手段及电化学基本理论知识。此综合实验通过前期文献调研、中期实验过程及后期实验结果分析,使学生将课堂学习的理论知识应用于实验过程,不仅加深了学生对理论知识的理解且拓宽了学生科学视野,培养了学生综合科研素养,提升学生绿色化学意识。A comprehensive electrochemical experiment was designed and introduced,S,N-CoMOF/CC electrocatalysts were prepared using a simple hydrothermal reaction and chemical immersion method.By characterizing the morphology and phase composition of the catalysts,as well as testing the electrocatalytic oxidation performance of 5-hydroxymethylfurfural(HMF),students gained a preliminary understanding of the preparation process,characterization methods of inorganic nanocomposites,and basic theoretical knowledge of electrochemistry.This comprehensive experiment involved preliminary literature research,mid-term experimental procedures and later experimental result analysis,enabled students to apply the theoretical knowledge learned in the class to the experimental process.It not only deepened students'understanding of theoretical knowledge,but also broadened their scientific perspective,cultivated their comprehensive scientific research literacy,and enhanced their awareness of green chemistry.

关 键 词：金属有机框架材料 电化学 HMF氧化 综合实验 科教融合 

分 类 号：G642.0[文化科学—高等教育学]