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出 处:《精细化工》1992年第1期34-36,共3页Fine Chemicals
摘 要:探讨了合成羟基香茅醛的反应条件。以脱水剂促进香茅醛与二乙醇胺缩合,生成稳定缩合物,产率达97.9%;缩合物的酸催化水合后的水解反应在保护剂存在下进行,羟基香茅醛的产率达87.7%。The reaction conditions of synthesizing hydro-xycitronellal have been explored . The condensation of citronellal with diethanolamine was promoted in the existence of dehydrating agent, producing a stable condensate, the yield was 97. 9%; After acid catalytic dehydration the condensate subsequent hydrolysis was proceeded in the existence of protective agent, the yield of hydroxycitronellal came up to 87.7%.
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