GC/MS法测定五加皮保健酒的挥发性特征成分  

Determination of Volatile Feature Components in Wujiapi Healthcare Wine by Gas Chromatography-Mass Spectrometry

作　　者：许荣年[1] 鲍忠定[1] 秦志荣[1] 陈青俊[1] 

机构地区：[1]浙江省轻工业研究所质量检验中心,浙江杭州310009

出　　处：《酿酒科技》2004年第2期95-96,共2页Liquor-Making Science & Technology

摘　　要：建立了用气相色谱-质谱联用法测定五加皮保健酒中桂皮醛、4-甲氧基水杨醛、丁香酚、藁本内酯、对甲氧基桂皮酸乙酯含量的方法,并对10个样品酒进行了检测。采用石油醚-乙醚提取法进行样品前处理,HPINNOWAX毛细管柱分离,离子法(SIM)定量。加标回收率均在91.6%以上。检测结果表明,五加皮保健酒中的挥发性特征成分含量在不同产品之间有较大差异。A gas chromatography-mass spectrometric method for det er mination of cinnamaldehyde,4-methoxysalicylaldehyde,eugenol,ligustilide and ethyl p-methoxycinnamate in Wujiapi healthcare wine was reported.10Wine sam ples were pretreated with petroleum ether-ether extraction,then analyzed throu gh HP INNOWAX column,and determined by selected ion method of mass spectrometry de-tector.The standard-added recovery rates were no less than91.6%.The determination result indicated that there was great difference of the volatile feature components among those wine samples.(Tran.by YUE Yang)

关 键 词：分析检测 气相色谱 质谱 五加皮保健酒 挥发性特征成分 

分 类 号：TS262[轻工技术与工程—发酵工程]