PERCHLORATE

作品数:85被引量:120H指数:6
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相关领域:理学更多>>
相关作者:刘晋湘梁蓓陈建军严伍启廖昕更多>>
相关机构:西安北方惠安化学工业有限公司北京理工大学南京理工大学中国科学技术大学更多>>
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相关基金:国家自然科学基金国家重点基础研究发展计划江苏省自然科学基金中国科学院科研项目更多>>
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Novel Perchlorate and Sulphate Salts of 2-Aminonicotinic Acid:Synthesis,Characterization,Thermal Studies and Hirshfeld Surface Analysis被引量:1
《Chinese Journal of Structural Chemistry》2016年第1期7-15,共9页马玉恒 葛书旺 沈亚 孙柏旺 
supported by the prospective joint research project of Jiangsu province(BY20122193);the Fundamental Research Funds for the Central Universities(CXZZ12_0119)
Since 2-aminonicotinic acid is a zwitterionic molecule,the salt or co-crystal strategy was used for the precipitation under identical conditions and obtained two novel salts: salt 1 with 2:1:2 stoichiometry of 2-am...
关键词:2-aminonicotinic acid salt X-ray diffraction Hirshfeld surfaces 
Unexpected Synthesis and Crystal Structure of Macrocyclic Nickel Complex Involving Rare S-Cl Bond
《Chinese Journal of Structural Chemistry》2013年第3期420-424,共5页欧光川 袁先友 李治章 
supported by the Science and Technology Planning Project of Hunan Province (2012FJ3050,2012NK3067);the Construct Program of the Key Discipline in Hunan Province (2011–76);the Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province (2012–318)
A novel complex of [NiL(OOCNH2C2H3SClO3)]·H2O was obtained unexpectedly by the reaction of [Ni(rac-L)](ClO4)2 with l-cysteine (L=5,5,7,12,12,14-hexamethyl-1,4,8,11-tetra- azacyclotetradecane), and characteriz...
关键词:macrocyclic nickel(Ⅱ) complexes crystal structure L-CYSTEINE PERCHLORATE 
Synthesis and Crystal Structure of Bis(2-acetylpyridine thiosemicarbazonato)-indium(iii) Perchlorate Hydrate
《Chinese Journal of Structural Chemistry》2011年第6期882-886,共5页王乐 边玮玮 朱凌 倪荣军 陶琳 
Financially supported from the Science Research Foundation of Shandong Entry-Exit Inspection;Quarantine Bureau (No. SK201042);Weifang Medical University (No. KQ2007030)
The title complex bis(2-acetylpyridine thiosemicarbazonato)-indium(iii) perchlo-rate hydrate has been synthesized by the reaction of 2-acetylpyridine thiosemicarbazide(L) with indium(iii) perchlorate,and its s...
关键词:self-assembly cationic complex polyatomic counterion HYDROGEN-BOND 
Crystal Structures of Schiff Base from 4-Aminoantipyrine and Pyridine-2-carboxaldehyde and Its Perchlorate
《Chinese Journal of Structural Chemistry》2008年第12期1506-1510,共5页谭明雄 刘冰 刘延成 陈振锋 周忠远 梁宏 
supported by the NSF of Guangxi Province (No. 0575046, 0575049);the Program for New Century Ten-Hundred-Thousand Excellent Talents of Guangxi (No. 2003223);the National Natural Science Foundation of China (No. 20361002, 30460153) as well as TRAPOYT;NCET-04-0836 of Chinese Ministry of Education
The Schiff base pyridine-2-carboxaldehyde-4-aminoantipyrine (CI7H16N4O 1) and its perchlorate (C17H17N4O·ClO4 2) have been prepared and characterized by elemental analysis, IR spectra and single-crystal X-ray cry...
关键词:crystal structure 4-AMINOANTIPYRINE pyridine-2-carboxaldehyde Schiff base 
Synthesis and Crystal Structure of 3,3'-Bis(2-benzimidazolyl)-2,2'-dipyridine with Hydrated Zinc(Ⅱ) Perchlorate
《Chinese Journal of Structural Chemistry》2007年第4期439-444,共6页苗少斌 吉保明 杜晨霞 
Supported by the National Natural Science Foundation of China (No. 20471054) ;the Henan Innovation Project for University Prominent Research Talents (No. 2005 KYCX021)
The reaction of Zn(ClO4)2·6H2O with 3,3'-bis(2-benzimidazolyl)-2,2'-dipyridine (L) gave a mononuclear zinc(Ⅱ) complex: [ZnL2](CIO4)2·2DMF·4H2O, which was structurally characterized by EA, IR, UV, ^1H ...
关键词:zinc perchlorate hexahydrate 3 3'-bis(benzimidazolyl)-2 2'-dipyridine crystal structure 
Synthesis and Crystal Structure of an Ion-pair Supramolecular Associate 2,9-Diformyl-1,10-phenanthrolinebis-(2,6-dimethylanil)cobalt(Ⅱ) Perchlorate被引量:3
《Chinese Journal of Structural Chemistry》2006年第7期861-865,共5页LI Gang JIE Su-Yun TANG Ning SUN Wen-Hua 
This work was supported by NNSFC (No. 20473099)
2,9-Diformyl-l, 10-phenanthrolinebis(2,6-dimethylanil)cobalt(Ⅱ) perchlorate was synthesized and demonstrated to be [COL2][ClO4]2 by X-ray diffraction analysis. It crystallizes in the monoclinic system, space grou...
关键词:1 10-PHENANTHROLINE cobalt complex crystal structure hydrogen bond 
Synthesis and Crystal Structure of 6-(3'-Indolyl)-8-(p-chlorophenyl)-10,10dimethyl-10H-pyrido [1,2-a] Indolium Perchlorate
《Chinese Journal of Structural Chemistry》2004年第12期1371-1375,共5页姜林 汪建民 李长城 
The synthesis of the title compound ([C28H22ClN2]·ClO4) has been synthesized and its structure was determined by X-ray diffraction. The compound belongs to the monoclinic system, space group P21/n with a = 15.113(5),...
关键词:pyrido [1 2-a] indolium perchlorate crystal structure SYNTHESIS MECHANISM 
Synthesis and Crystal Structure of Bis(p-aminotoluene)-bis(dimethylglyoximato) Cobalt(Ⅲ) Perchlorate
《Chinese Journal of Structural Chemistry》2003年第3期255-259,共5页陈丽娟 林深 杨明星 刘世雄 
This work was supported by the foundation for University Key Teacher by the Ministry of Education and the foundation for Innovative Youth of Fujian province (No 2002J001)
The title compound (C22H32.5ClCoN6O8.25, Mr = 607.42) crystallizes in the orthor- hombic system, space group C2221 with a = 11.320(2), b = 20.933(4), c = 23.936(5) ? V = 5672(2) 3, Dc = 1.423 g/cm3, Z = 8, m(MoKa) = 0...
关键词:cobalt complex DIMETHYLGLYOXIME crystal structure 
Synthesis and Crystal Structure of the Perchlorate Salt of Diprotonated 2,3-Di-2-pyridyl-5-nitroquinoxaline
《Chinese Journal of Structural Chemistry》2002年第6期621-625,共5页XUQiang BUXian-He  
This work was financially supported by NNSFC(No.29971019)
The diprotonated perchlorate salt of 2,3-di-2-pyridyl-5-nitroquinoxaline [C18H13N5O2](ClO4)2·(CH3OH)·(C2H5OH) has been synthesized and characterized by elemental analysis, IR and NMR spectra. X-ray diffraction analy...
关键词:synthesis crystal structure polypyridyl compound proton-sponge 
The Crystal Structure of 1, 4, 7, 10- Tetraazacyclododecane Hydrate Triperchlorate
《Chinese Journal of Structural Chemistry》1998年第4期293-295,共3页KONG De-Yuan XIE Yu-Yuan ZHU Qin  XIE Yu-Li(Shanghai Institute of Material Medica, the Chinese Academy of Sciences,No. 294, Taiyuan Road, Shanghai 200031, China)HUANG Xiao-Ying(Fujian Institute of Research on the Structure of Matter,the Chinese Academy 
The title complex [(C8H23N4)3+ (ClO4)3-]. H2O was crystallized intriclinic system, P1 space group with unite cell parameters: a= 8. 386(2), b= 10. 558(2), c=11. 865(3) A, a= 77. 75(2)’ β= 72. 65(2),γ= 74. 77(2)°, ...
关键词:crystal structure tetraazacyclododecane PERCHLORATE HYDRATE 
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