TETRAHYDROPYRANYLATION

作品数:8被引量:10H指数:2
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相关领域:理学更多>>
相关期刊:《International Journal of Organic Chemistry》《Chinese Journal of Catalysis》《Chinese Journal of Chemistry》《Chinese Chemical Letters》更多>>
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Selective Monoprotection of Symmetrical Diols in a Flow Reactor
《International Journal of Organic Chemistry》2018年第2期264-271,共8页Hisashi Masui Masaru Takizawa Yuki Sakai Yasuhiro Kajiwara Kiyofumi Wanibuchi Mitsuru Shoji Takashi Takahashi 
Desymmetrization reactions provide a powerful approach for the construction of complex molecules. Various methods have been developed for the selective monoprotection of symmetrical diols;however, their application to...
关键词:DESYMMETRIZATION SELECTIVE Monoprotection FLOW Synthesis DIOLS TETRAHYDROPYRANYLATION 
{[K.18-Crown-6]Br_3}_n:A tribromide catalyst for the catalytic protection of amines and alcohols
《催化学报》2013年第9期1730-1733,共4页Gholamabbas Chehardoli Mohammad Ali Zolfigol Fateme Derakhshanpanah 
support for this work from the research affairs of Hamedan University of Medical Sciences,Hamedan,I.R.Iran;partial support of this work by the Research Affairs Office of Bu-Ali Sina University;Center of Excellence in Development of Chemical Method(CEDCM)Hamedan,I.R.Iran
{[K.18-Crown-6]Br3}n,a unique tribromide-type catalyst,was utilized for the N-boc protection of amines and trimethylsilylation(TMS)and tetrahydropyranylation(THP)of alcohols.The method is general for the preparation o...
关键词:{[K.18-Crown-6]Br3}n TRIMETHYLSILYLATION TETRAHYDROPYRANYLATION Alcohol Organic TRIBROMIDE N-boc PROTECTION of amine 
Tetrahydropyranylation of Alcohols and Phenols Using Poly- styrene Supported Lewis Acids as Catalysts
《Chinese Journal of Chemistry》2012年第10期2567-2572,共6页张毅 窦倩倩 刘员 戴立言 王晓钟 陈英奇 
Polystyrene supported TiCI4 (Ps-TiCI4) and polystyrene supported FeC13 (Ps-FeC13) were prepared by coordi- nating Lewis acids with polystyrene. The catalysts were characterized by TGA, BET, SEM, IR and pyri- dine-...
关键词:tetrahydropyranylation/detetrahydropyranylation Ps-TiC14 Ps-FeCI3 polystyrene supported Lewisacids 
Efficient and green tetrahydropyranylation and deprotection of alcohols and phenols by using activated carbon supported sulfuric acid被引量:2
《Chinese Chemical Letters》2008年第8期893-896,共4页Jin Hui Yang Xuan Zhang Wan Yi Liu 
the special research project of the National 973 Foundation of China(No.2006CB708606);the National Natural Science Foundation of China(No.20562010)
A simple, green and efficient method for the DHP protection of various alcohols and phenols and the subsequent removal of the corresponding protective group in the presence of a catalytic amount of the activated carbo...
关键词:TETRAHYDROPYRANYLATION DEPROTECTION THP ethers Activated carbon 
Copper methanesulfonate-acetic acid as a novel catalytic system for tetrahydropyranylation of alcohols and phenols被引量:7
《Chinese Chemical Letters》2007年第7期799-802,共4页Min Wang Zhi Guo Song Hong Gong Heng Jiang 
A synergistic catalytic effect between copper methanesulfonate and acetic acid in tetrahydropyranylation of alcohols and phenol at room temperature under solvent free condition has been described. Both alcohols (prim...
关键词:TETRAHYDROPYRANYLATION Synergistic effect Copper methanesulfonate Acetic acid 
Regioselective tetrahydropyranylation of alcohols catalyzed by Fe(HSO_4)_3被引量:4
《Chinese Chemical Letters》2007年第7期803-806,共4页Farhad Shirini Mohammad Ali Zolfigol Abdol-Reza Abri 
Alcohols are selectively and efficiently protected as their tetrahydropranyl ethers in the presence of a catalytic amount of Fe(HSO4)3 in good to high yields. All reactions are performed under mild and completely he...
关键词:ALCOHOLS TETRAHYDROPYRANYLATION Tetrahydropyranyl ethers Fe(HSO4)3 Heterogeneous reaction conditions 
GaI_3 Catalyzed Tetrahydropyranylation of Alcohols and Phenols被引量:2
《Chinese Journal of Chemistry》2004年第11期1341-1343,共3页孙培培 胡志新 
Project supported by the Natural Science Foundation of the Education Department of Jiangsu province (No. 03KJD150109).
In dichloromethane, the nucleophilic addition of alcohols or phenols to 3,4-dihydro-2H-pyran (DHP) was cata-lyzed effectively by gallium triiodide which was generated in situ by the reaction of gallium metal and iodin...
关键词:gallium triiodide alcohol or phenol 2-alkoxy(aryloxy)tetrahydropyran the protection of hydroxyl group 
A Mild and Practical Procedure for Tetrahydropyranylation of Alcohols and Phenols Catalysed by Anhydrous Ferrous Sulfate
《Chinese Chemical Letters》1998年第3期241-244,共4页Li, TS Zhang, ZH Jin, TS Li, YL 
An easy preparation of tetrahydropyranyl (THP) ethers of alcohols and phenols with 3,4-dihydro-2H-pyran (DHP) in refluxing dichloromethane has been carried out in good to excellent yields under catalysis of anhydrous ...
关键词:preparation tetrahydropyranyl ethers protection of hydroxy catalysis anhydrous ferrous sulfate 
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