REAGENT

作品数：370被引量：405H指数：8
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  • 期刊=Chinese Journal of Structural Chemistryx
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Mild-temperature Synthesis of Covellite Copper Sulfide Hexagonal Nanoplatelets via the Hydrothermal Route
《Chinese Journal of Structural Chemistry》2009年第1期19-24,共6页丁同勇 郭国聪 王明盛 陈其湧 周薇薇 黄锦顺 
supported by the NNSFC (20701037);the NSF of Fujian Province (2006J0013);Fund of Fujian Key Laboratory of Nanomaterials (2006L2005)
Covellite CuS hexagonal nanoplatelets were prepared by a simple hydrothermal process at mild temperature, using sodium dodecyl benzene sulfonate （SDBS） as an assisting reagent. The products were characterized by X-r...
关键词：hydrothermal route copper sulfide hexagonal nanoplatelets assisting reagent 
Synthesis and Crystal Structure of 3,5-Diphenyl-1,2-di(4-chlorophenyl)pyrrole
《Chinese Journal of Structural Chemistry》2005年第11期1314-1317,共4页SHI Da-Qing SHI Chun-Ling ZHUANG Qi-Ya 
This work was supported by the Natural Science Foundation of Jiangsu Education Department (No. 03KJB 150136)
The title compound （C28H19Cl2N） has been synthesized by the reaction of dibenzoylmethane and N-（4-chlorobenzylidene）-4-chlorobenzenamine promoted by low-valent titanium reagent, and characterized by elemental anal...
关键词：PYRROLE low-valent titanium reagent crystal structure 
Crystal Structures and Antimicrobial Activity of Two Phosphorus Compounds
《Chinese Journal of Structural Chemistry》2005年第10期1211-1216,共6页SHEN Xiao-Qing LIU Hong-Lei ZHANG Hong-Yun ZHANG Hong-Quan MAO Hong-Yan WU Qing-An ZHU Yu HOU Hong-Wei 
This work was supported by the National Natural Science Foundation of China (20271046), Natural Science Foundation of Henan Education Department (2004150004) and Natural Foundation of Henan Province (200011500027)
One phosphorus heterocycle compound 1, C13H13N2OPS, was synthesized by the reaction of Lawesson＇s reagent （LR） with o-phenylene diamine. The crystal belongs to the orthorhombic system, space group P212121 with a = ...
关键词：Lawesson＇s reagent ring-closure reaction PHOSPHORUS crystal structure 
Synthesis and Structure of Ag(I)- Containing Coordination Polymers Based on Quaternary Ammonium Template Reagent被引量：1
《Chinese Journal of Structural Chemistry》2005年第5期509-512,489,共5页柯子厚 陈之荣 李浩宏 黄长沧 肖光参 赵斌 
This work was supported by the Foundation of Education Committee of Fujian Province (JB03053, JB04016)
A novel coordination polymer [(C8H20N)(Ag2I3)]n ([C8H20N]+ = tetraethyl ammo- nium (TEA)) was synthesized by the reaction of AgI and C8H20NI at room temperature with pH = 6.5, and structurally characterized by means o...
关键词：coordination polymers template synthesis IODIDE quaternary ammonium 
Synthesis and Crystal Structure of 1-(o-methylphenyl)-2-(p-methoxyphenyl)-1,3,2-diazaphospholidin-4-thione-2-sulfide
《Chinese Journal of Structural Chemistry》1997年第3期215-218,共4页HE Liang-Nian  CHEN Ru-Yu ZHOU Jia(Institute of Elemento-Organic Chemistry, National Key Laboratory ofElemento - Organic Chemistry, Nankai University, Tianjin, 300071)WANG Hong-Gen YAO Xin-Kan(Central Laboratory, Nankai University, Tianjin, 300071) 
The crystal structure of the title compound C16H17N2OPS2, has beendetermined by single-crystal X-ray diffraction at 299K. The crystal is monoclinic withspace group P21/n, a=9. 549(2), b= 7- 954(5), c=23. 039(8) A, β=...
关键词：phosphorus HETEROCYCLE Lawesson’s REAGENT crystal structure herbicidal activity 
Crystal Structure of N-Phenylisothiocyanatido-Phosphonamidothioate
《Chinese Journal of Structural Chemistry》1997年第3期200-202,共3页HE Liang-Nian  CHEN Ru-Yu(Institute of Elemento-Organic Chemistry, Nankai University, Tianjin 300071)WANG Hong-Gen YAO Xin-Kan(Central Laboratory, Nankai University, Tianjin 300071) 
The crystal structure of the title compound, C14H13N2OPS2, has beendetermined by single crystal X-ray diffraction at 299(±1 )K. The crystal is monoclinicwith space group P21/n, a= 11. 310(2), b=8. 363(3), c= 16. 847(...
关键词：isothiocyanatidophosphonamidothioate crystal structure Lawesson's reagent 
Assignation of Acidic Dissociation Constants of Dimethoxyphenylfluorone and Dibromodimethylaminophenylfluorone
《Chinese Journal of Structural Chemistry》1996年第4期297-300,共4页陈天明 王东进 等 
The acidic dissociation constants of dimethoxyhenylfluorone (DMOPF)and dibromo-dimethylaminophenylflurone(Br_2-DMAPF) were determined from a spectrophotometric study, with the results as follows:DMOPF: pk_1=2. 68 pk_2...
关键词：dissociation constant assignation organic reagent SPECTROPHOTOMETRY Hückel molecular orbital method 
Synthesis and Crystal Structure of 1, 5-Bis( 1'-phenyl-3'-methyl- 5'-pyrazolone- 4') -1- ( 4'-aminobutand-1'-imino) -5-pentaneone被引量：2
《Chinese Journal of Structural Chemistry》1995年第2期117-121,共5页杨鲁勤 王宏根 等 
The title compound of PhCH_3C_3HN_2 (O )C (O) (CH_2) _3C [N (CH_2 )_4 NH_2]C_3HN_2 (O)CH_3Ph (L), a new Schiff-base containing diketone, has been synthesized. Its crystal structure has been determined by X-ray diffrac...
关键词：SCHIFF-BASE DIKETONE crystal structure fluorescence reagent 
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