HS-SPME/GC-MS法分析树莓饮品中挥发性成分  

Analysis of the volatile components in the drink made from raspberry by HS-SPME/GC-MS

作　　者：孙慧玲[1] 王佳佳[1] 穆思蒙[2] 王微[1] 许启泰[1] 邢晗[1] 康文艺[1] 

机构地区：[1]河南大学中药研究所,河南开封475004 [2]沈阳药科大学药学院,辽宁沈阳110016

出　　处：《河南大学学报（医学版）》2012年第3期223-224,共2页Journal of Henan University:Medical Science

基　　金：河南省科技厅重点攻关项目(112102310310)

摘　　要：目的分析树莓饮品中的挥发性成分。方法采用顶空固相微萃取和气质联用技术(HS-SPME/GC-MS),结合保留指数法并用峰面积归一化法测定相对百分含量。结果共鉴定出2种挥发性成分,相对含量占挥发性成分总峰面积的98.3%。结论主要挥发性成分为脱氢醋酸(95.34%)和2-乙基-3-羟基-4H-吡喃-4-酮(2.96%)。Objective To search the volatile components of the drink made from raspberry in Fengqiu County,Henan Province in China.Methods The volatiles were analyzed by head-space solid micro-extraction,coupled with GC/MS and Kovats induce.Results The relative content for the 2 identified compounds accounted for 98.3% of the total essential constituents.Conclusion The major volatile components were 4H-pyran-4-one,2-ethyl-3-hydroxy-（95.34%）,dehydroacetic acid（2.96%）.

关 键 词：树莓饮品 挥发性成分 固相微萃取 气相色谱-质谱 

分 类 号：R284.1[医药卫生—中药学]