响应面法优化多香果油树脂超声波提取工艺  

Optimization of Ultrasonic Extraction Process of Allspice Oleoresin by Response Surface Methodology

作　　者：刘煜宇 连培康 郭伟康 包秀萍 罗建飞 陈联明 LIU Yuyu;LIAN Peikang;GUO Weikang;BAO Xiuping;LUO Jianfei;CHEN Lianming(Yunnan Reascend Tobacco Technology(Group)Co.,Ltd.,Kunming 650106;Jiangxi China Tobacco Industry Co.,Ltd.,Nanchang 330096;Ganzhou Cigarette Factory of China Tobacco Jiangxi Industrial Co.,Ltd.,Ganzhou 341000)

机构地区：[1]云南瑞升烟草技术(集团)有限公司,昆明650106 [2]江西中烟工业有限责任公司,南昌330096 [3]江西中烟工业有限责任公司赣州卷烟厂,赣州341000

出　　处：《食品工业》2022年第4期76-81,共6页The Food Industry

摘　　要：以多香果油树脂提取率为考察指标,采用响应面法优化超声波提取工艺,并用气相色谱-质谱仪进行分析和鉴定挥发性成分。最佳提取条件为超声波频率64 kHz、提取温度58℃和提取时间56 min,提取率为13.45%。共鉴定出77种致香成分,主要为丁子香酚8927.616μg/g(对照59.403μg/g)、甲基丁香酚9630.215μg/g(对照72.769μg/g)、α-松油醇1309.413μg/g(对照15.413μg/g)。优化工艺能显著提高多香果油树脂中的致香成分含量。The extraction rate of allspice oleoresin taken as the index,a response surface method experiment was conducted to optimize the ultrasonic extraction process.Volatile components were analyzed and identified via gas chromatography-mass spectrometry.The optimal extraction condition was ultrasonic frequency 64 kHz,extraction temperature 58℃ and extraction time 56 min,and extraction rate of 13.45%.About 77 peak compounds were isolated and identified.The main volatile components were eugenol 8927.616μg/g(CK 59.403μg/g),methyl eugenol 9630.215μg/g(CK 72.769μg/g)andα-terpineol 1309.413μg/g(CK 15.413μg/g).The optimal ultrasonic extraction process could effectively improve the content of volatile components in allspice oleoresin.

关 键 词：多香果油树脂 超声波提取工艺 响应面法 气相色谱-质谱法 挥发性成分 

分 类 号：O657.63[理学—分析化学] TS264[理学—化学]