食品抗氧剂芝麻酚的合成研究  

Synthesis Research of Sesamol as Food Antioxidant

作　　者：张洋 魏锦健 单绍军 Zhang Yang;Wei Jinjian;Shan Shaojun(College of Pharmaceutical and Chemical Engineering,Guangdong Pharmaceutical University,Zhongshan Guangdong 528458;Guangdong Cosmetics Engineering&Technology Research Center,Zhongshan Guangdong 528458)

机构地区：[1]广东药科大学医药化工学院,广东中山528458 [2]广东省化妆品工程技术研究中心,广东中山528458

出　　处：《山西化工》2023年第2期5-6,共2页Shanxi Chemical Industry

基　　金：广东省大学生创新创业训练计划项目(S202110573009)。

摘　　要：本文以胡椒环为原料,首先制备3,4-亚甲二氧基苯乙醇酸,接着以国内未见报道的氯化铜为催化剂氧化3,4-亚甲二氧基苯乙醇酸制得胡椒醛,然后以30%的双氧水为氧化剂,经过氧化得到芝麻酚。该合成方法工艺简单,反应条件温和,产品三步总收率为52.8%。3,4-Dioxymethylene was prepared from 1,3-Benzodioxole.Heliotropin was prepared from 3,4-dioxymethylene by oxidation with CuCl_(2),then sesamol was synthesized from heliotropin by oxidation of 30%H_(2)O_(2).The method has several advantages,such as mild reaction condition,convenient operation and the total yield is 52.8%.

关 键 词：芝麻酚 胡椒醛 合成 食品抗氧剂 

分 类 号：TS205[轻工技术与工程—食品科学]