玫瑰净油挥发性香味的成分分析  

Analysis of Volatile Components of Rose Essential Oil by Headspace Solid Phase Microextraction Gas Chromatography Mass Spectrometry

作　　者：潘文亮 段旭瑞 王蕊 王翰书 张逸寒 PAN Wenliang;DUAN Xurui;WANG Rui;WANG Hanshu;ZHANG Yihan(Technology Center,China Tobacco Hebei Industrial Co.,Ltd.,Shijiazhuang 050051,China;College of Tobacco Science and Engineering,Zhengzhou University of Light Industry,Zhengzhou 450001,China)

机构地区：[1]河北中烟工业有限责任公司技术中心,河北石家庄050051 [2]郑州轻工业大学烟草科学与工程学院,郑州450001

出　　处：《云南化工》2025年第3期62-65,共4页Yunnan Chemical Technology

基　　金：河北中烟工业有限责任公司重点项目(HBZY2024A039)。

摘　　要：【目的】为了分析玫瑰净油中的挥发性成分。【方法】采用顶空固相微萃取-气相色谱质谱法测定玫瑰净油中的挥发性成分。【结果】①玫瑰净油中共检测出88种挥发性成分,包括烯烃类30种,酯类19种,烷烃类7种,醇类10种,酚类6种,醛类5种,芳香烃类4种,酮类3种,酸类2种,醚类1种;②挥发性成分中醇类质量分数占比最多(56.15%),酮类质量分数占比最少(0.13%);③玫瑰净油中质量分数较高的物质有苯乙醇(46.83%)、丁香酚(22.64%)、橙花醇(3.07%)、4-烯丙基苯酚(2.46%)、甲基丁香酚(1.83%)、芳樟醇(1.78%)、水杨酸甲酯(1.50%)。【结论】可为开发利用玫瑰净油提供参考。[Objective]To analyze the volatile components in rose oil.[Method]The volatile components in rose essential oil were analyzed by headspace solid phase microextraction with meteorological chromatography mass spectrometry.[Results]The results showed as follows:(1)A total of 88 volatile components were detected in rose oil,including 30 olefins,19 esters,7 alkanes,10 alcohols,7 phenols,5 aldehydes,4 aromatic hydrocarbons,3 ketones,2 acids and 1 ether;(2)The contents of alcohols accounted for the most(56.15%)and ketones accounted for the least(0.13%);③The high content substances in rose oil were methyl salicy late(1.50%),linalool(1.78%),phenylethanol(46.83%),3,7-dimethyl-2,6-octdiene-1-ol(3.07%),4-allyl phenol(2.46%),2-methoxy-3-(2-allyl)-phenol(22.47%)and methyl Eugenol(1.83%).[Conclusion]It can provide reference for the development and utilization of rose oil.

关 键 词：玫瑰净油 挥发性成分 顶空固相微萃取 气相色谱-质谱联用 成分分析 

分 类 号：TQ651.2[化学工程—精细化工]