the National Basic Research Program of China 973 Program(No.2003CB114400);the National Natural Science Foundation of China(No.20476098);for financial support.(No.20676123)
A mild and simple method for the synthesis of dialkyl chlorophosphates is described, bis(trichloromethyl) carbonate (BTC) is used as the effective reagent for the conversion of dialkyl phosphites to their correspo...