DIAZEPINE

作品数:18被引量:5H指数:1
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相关领域:理学化学工程更多>>
相关机构:上海应用技术大学更多>>
相关期刊:《Journal of Zhejiang University-Science B(Biomedicine & Biotechnology)》《Chinese Journal of Chemistry》《Journal of Hainan Medical University》《Defence Technology(防务技术)》更多>>
相关基金:国家自然科学基金河北省自然科学基金更多>>
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  • 期刊=Chinese Chemical Lettersx
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Highly efficient one-pot,three-component synthesis of1,5-benzodiazepine derivatives被引量:1
《Chinese Chemical Letters》2014年第2期327-332,共6页Xiao-Qing Li Lan-Zhi Wang 
financial support from the National Natural Science Foundation of China(No.21276064);the Natural Science Foundation of Hebei Education Department(No.2008320);the Science Foundation of Hebei Normal University(No.2011Y04)
A general, mild and efficient protocol for the synthesis of ethyl 4-methyl-2-(thiophen)-2,5-dihydro-1,5- benzodiazepine-3-carboxylate is achieved for first time using H3PMo12O40 in ethanol at 0 ℃ by a one- pot, th...
关键词:ONE-POT Synthesis 1 5-Benzodiazepine derivative 
An efficient synthesis of 1,5-benzodiazepine derivatives catalyzed by boric acid被引量:2
《Chinese Chemical Letters》2009年第8期905-908,共4页Xin Zhou Mei Yue Zhang Shu Tao Gao Jing Jun Ma Chun Wang Chao Liu 
1,5-Benzodiazepine derivatives have been synthesized by the condensation of o-phenylenediamines and ketones in the presence of boric acid as catalyst under mild conditions. This method is simple, environmentally benig...
关键词:1 5-Benzodiazepincs O-PHENYLENEDIAMINES Boric acid Synthesis 
Novel,efficient,and green procedure for the synthesis of 1,5-benzodiazepines catalyzed by MgBr_2 in aqueous media被引量:1
《Chinese Chemical Letters》2009年第1期32-36,共5页Shivaji S.Pawar Murlidhar S.Shingare Shivaji N.Thore 
MgBr2 performs as a novel catalyst for the synthesis of various 1,5-benzodiazepine derivatives from wide range of substituted o- phenylenediamines and various ketones in good to excellent isolated yields (93-98%) us...
关键词:MgBr2 O-PHENYLENEDIAMINES KETONES Aqueous media 1 5-Benzodiazepine 
Sulfanilic acid catalyzed solvent-free synthesis of 1,5-benzodiazepine derivatives
《Chinese Chemical Letters》2007年第11期1305-1308,共4页Jaiprakash N.Sangshetti Nagnnath D.Kokare Devanand B.Shinde 
Sulfanilic acid has been found to be an efficient catalyst for the synthesis of 1,5-benzodiazepines from o-phenylenediamine and ketones. This method is simple, effective and environmentally friendly and gives better y...
关键词:1 5-Benzodiazepines Sulfanilic acid catalyst Solvent free condition 
New Approach to Synthesis of Tetrahydroisoquino[2,l-c] [1,3]-benzodiazepine
《Chinese Chemical Letters》2004年第7期759-761,共3页HongMinMA ZhanZhuLIU ShiZhiCHEN XiaoTianLIANG 
A concise and efficient synthesis of the new compounds tetrahydroisoquino [2,1-c] [1,3] benzodiazepine 5 and 7 is reported.
关键词:TETRAHYDROISOQUINOLINE Mannich reaction BENZODIAZEPINE berberine. 
Facile Synthesis of 1,2-Diazepine Derivatives under Microwave Irradiation
《Chinese Chemical Letters》2004年第3期284-285,共2页JinXianWANG XiaoNingSHI KeHuWANG XiuQinMEN 
An efficient and convenient synthesis of 3, 5, 7-triaryl-4H-1, 2-diazepine from 2, 4, 6-triarylpyrylium salts and hydrazine in water under microwave irradiation is reported. The same reaction can be conducted using 2,...
关键词:Triarylpyryliums HYDRAZINE 1 2-diazepine derivatives microwave irradiation. 
Synthesis of 5-Substituted Hexahydro-1H-1, 4-Diazepine Analogues
《Chinese Chemical Letters》2001年第11期951-954,共4页Jing Shan SHEN Li Jun LEI Hai Fang MAO Jian Feng LI Ru Yun JI 
5-Substituted hexahydro-1H-1,4-diazepine analogues were synthesized starting from N,N'-dibenzyl-1, 2-ethylenediamine and methyl 2, 4-dibromide butyrate through nucleophilic substitution, reduction, chlorination, deben...
关键词:5-substituted hexahydro-1H-1 4-diazepine analogues synthesis bioactivity 
Synthesis of 2-Substituted Hexahydro-1H-1,4-diazepine Analogues
《Chinese Chemical Letters》2001年第3期193-194,共2页Jing Shan SHEN Li Jun LEI Tie Ma YAN Jian Feng LI Hui Jun LI Zhen Hua LI Ru Yun JI 
the Shanghai Development Fund of Science and Technology.
substituted hexahydro-1H-1,4-diazepine analogues were synthesized starting from N,N?-dibenzyl-1,3-propylene diamine and methyl-2,3-dibromo propionate through nucleophilic substitution, reduction, chlorination and debe...
关键词:Hexahydro-1H-1 4-diazepine analogues synthesis nucleophilic substitution reduction chlorination debenzylation. 
NEW HETEROCYCLIC SYSTEM SYNTHESIS VI. THE CYCLOADDITION DERIVATIVES OF 1,5-BENZOTHIAZEPINE AND 1,5-BENZODIAZEPINE被引量:1
《Chinese Chemical Letters》1994年第7期557-560,共4页Jia Xi XU Sheng JIN(Department of Chemistry, Peking University, Beijing 100871) 
Dihydro-1H-1, 5-benzodiazepines and 1-benzoy1-2, 3-dihydro-1H-1H-1,5-benzodiazepines react with .α-carbonylkelenes, generated from 2-diazo-1,3-diphenyl-1,3-propandione or 2-diazo-1-phenyl-1,3-butandione by heating, t...
关键词:VI SYNTHESIS CYCLOADDITION SYSTEM HETEROCYCLIC AND BENZODIAZEPINE 
NEW HETEROCYCLIC SYSTEM SYNTHESIS III REACTIONS OF 1,2-DIHYDRO-2,4-DISUBSTITUTED-1,5-BENZODIAZEPINE WITH DICHLOROCARBENE
《Chinese Chemical Letters》1992年第3期179-180,共2页Xin Yu ZHANG Sheng JIN Ren An LIAO 
Three kinds of products have been separated from the reaction mixtures of 1,2-dihydro-2, 4-disubstituted-1,5-benzodiazepine with: CCI_2.Besides the addition products of: CCI_2 to C=N.the inserted products of: CCI_2 to...
关键词:CCI Pro NEW HETEROCYCLIC SYSTEM SYNTHESIS III REACTIONS OF 1 2-DIHYDRO-2 4-DISUBSTITUTED-1 5-BENZODIAZEPINE WITH DICHLOROCARBENE III 
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