REAGENT

作品数：370被引量：405H指数：8
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相关机构：北京大学武汉大学中南大学华东师范大学更多>>
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Rongalite as a Versatile Reagent in Organic Synthesis被引量：2
《Chinese Journal of Chemistry》2023年第23期3388-3400,共13页Huai-Yu Wang Xiang-Long Chen Yan-Dong Wu An-Xin Wu 
financial support from the the National Natural Science Foundation of China(Grants 21971080,21971079,21772051);supported by 111 Project B17019.
This review provides a comprehensive summary of progress to date in the utilization of rongalite as a versatile reagent in organic synthesis,with a focus on recent researches.The contents have been organized according...
关键词：RONGALITE Synthetic methods C1 building blocks Sulfone source Single electron donor Reductant 
Design, Synthesis and Application of a Robust d_(3)-Methyithiolating Reagent
《Chinese Journal of Chemistry》2023年第22期3045-3049,I0002,共6页Yanyang Zhang Yishuo Ren Jian Zhang Shaoli Liu Yahui Li 
financial support from the National Natural Science Foundation of China(22101005);the National Key Research and Development Program of China(2021YFD1700104);Key R&D Projects of Anhui Province(202104a06020008);Excellent Youth Program of Anhui Province(2022AH030095).
A deuterated methylthiolating reagent with a broad spectrum,designated as DMTp,has been ingeniously formulated.This new reagent can be produced with high efficiency through the simple combination of commercially avail...
关键词：New reagent d_(3)-Methylthiolating reagent Metal-catalyzed Application Aryl halides C1 building blocks Cleavage reactions Organohalides 
Practical Synthesis of NFSI Derivatives through ArSO_(2) NHF without F_(2)
《Chinese Journal of Chemistry》2022年第24期2956-2962,共7页Yu-Yang Zhang Xiu-Hua Xu Feng-Ling Qing 
The National Natural Science Foundation of China(21991211);the National Key Research and Development Program of China(2021YFF0701700)are greatly acknowledged for funding this work.
N-Fluorobenzenesulfonimide (NFSI) is one of the most popular fluorine-containing reagents for fluorination, imidation, sulfonylation, and oxidation reactions. Consequently, a variety of NFSI derivatives were designed ...
关键词：FLUORINE Fluorinating reagent SULFONAMIDES Synthetic methods DESULFONYLATION NFSI CONDENSATION 
Togni-ⅡReagent Mediated Selective Hydrotrifluoromethylation and Hydrothiolation of Alkenes
《Chinese Journal of Chemistry》2021年第12期3429-3434,共6页Shuang Teng Lingkui Meng Bingbing Xu Guangsheng Tu Peng Wu Zhiwen Liao Yulin Tan Jian Guo Jing Zeng Qian Wan 
Financial support from the National Natural Science Foundation of China(21877043,21702068,22025102);Wuhan Creative Talent Development Fund,and Fundamental Research Funds for the Central Universities(2017KFYXJJ150)is greatly appreciated;We also thank Analytical and Testing Center of HUST for NMR tests.
Based on the redox reactions of Togni-Ⅱreagent and thiols,a thiol-tuned selective functionalization of unactivated olefins was disclosed.In combination with aryl thiols,stoichiometric amount of Togni-Ⅱreagent prompt...
关键词：Togni-Ⅱreagent Hydrotriflupromethylation Thiol-ene reaction ALKENES Radical reactions 
S-Trifluoroethyl Benzenesulfonothioate:A Bench-Stable Reagent for Electrophilic Trifluoroethylthiolation被引量：1
《Chinese Journal of Chemistry》2020年第12期1625-1628,共4页Shuai Huang Ziheng Xi Kui Lu Haifeng Lu Chen-Ho Tung Zhenghu Xu 
We are grateful for financial support from the Natural Science Foundation of China and Shandong province(Nos.21971149,ZR2018MB010,ZR2019ZD45,ZR2017MB033);the Key Researchand Development Program of Shandong Province(No.2017CXGC1113);Tang scholar award and the Fundamental Research Funds of Shandong University.
of main observation and conclusion We report herein a practical approach for synthesis of an electrophilic trifluoroethylthiolation reagent PhSO2SCH2CF3(1)from easily available materials.The reaction proceeded through...
关键词：materials. REAGENT SUBSTITUTION 
Monofluoromethyl-Substituted Sulfonium Ylides:Preparation,Structure-Reactivity Study and Substrate Scope被引量：2
《Chinese Journal of Chemistry》2020年第11期1317-1331,共15页Xin Hong Yafei Liu Long Lu Qilong Shen 
The authors gratefully acknowledge the financial support from the National Natural Science Foundation of China(21625206,21632009,21421002);the Strategic Priority Research Program of the Chinese Academy of Sciences(XDB20000000)for financial support.
of main observation and conclusion Structure-reactivity study of a family of electrophilic monofluoromethylating reagents based on sulfonium ylide skeleton with different steric hindrance and electron-withdrawing prop...
关键词：BACKBONE REAGENT REACTIVITY 
Radical Heteroarylalkylation of Alkenes via Three-Component Docking-Migration Thioetherification Cascade被引量：3
《Chinese Journal of Chemistry》2020年第8期803-806,共4页Tao Niu Jige Liu Xinxin Wu Chen Zhu 
C.Z.is grateful for the financial support from the NationalNatural Science Foundation of China(Nos.21722205,21971173);the Project of Scientific and Technologic Infrastructure of Suzhou(SzS201905);the Priority Academic Program Development of Jiangsu Higher Education Institutions(PAPD).
A novel,rational-designed approach to access various heteroaryl-substituted alkyl thioethers was developed via docking-migration cascade process.By utilizing three components involving alkene,dual-function reagent,and...
关键词：process REAGENT ALKYLATION 
A Modular Synthesis of Antitumor Macrolide (-)-Lasonolide A被引量：1
《Chinese Journal of Chemistry》2020年第7期725-736,共12页Lin Yang Zuming Lin Kuan Zheng Luyao Kong Ran Hong 
the Drug Innovation Major Project(2018ZX09711001-005);the National Natural Science Foundation of China(91856202);the National Key R&D Program of China(2019YFA09005000);the Strategic Priority Research Program(XDB20000000);the Key Research Program of Frontier Sciences(QYZDYSSWSLH026)of the Chinese Academy of Sciences is highly appreciated.We also thank Jie Sun(SIOC,CAS)for the X-ray analysis.
Lasonolide A was identified as a potent antitumor macrolide towards various cancer cell lines.The two tetrahydropyrans bearing multiple stereogenic centers as well as the polyvene linkage attracted a dozen synthetic r...
关键词：ALDEHYDES LINKAGE REAGENT 
Chen's Reagent: A Versatile Reagent for Trifluoromethylation,Difluoromethylenation, and Difluoroalkylation in Organic Synthesis被引量：7
《Chinese Journal of Chemistry》2020年第2期202-212,共11页Qiqiang Xie Jinbo Hu 
the National Basic Research Program of China(Nos.2015CB931900,2016YFB0101200);the National Natural Science Foundation of China(Nos.21632009,21421002);the Key Programs of the Chinese Academy of Sciences(No.KGZD-EWT08);the Key Research Program of Frontier Sciences of CAS(No.QYZDJ-SSW-SLH049);Shanghai Science and Technology Program(No.18JC1410601)is acknowledged。
Methyl fluorosulfonyldifluoroacetate(FSO2CF2CO2Me or MFSDA),often called"Chen's reagent",is commonly used to synthesize trifluoromethylated and difluoroalkylated compounds.This important reagent was initially develope...
关键词：compounds. REAGENT REAGENT 
Advances in Enantioselective Construction of Trifluoromethoxylated Stereogenic Carbon Centers被引量：2
《Chinese Journal of Chemistry》2020年第1期101-102,共2页Xiaohuan Jiang Pingping Tang 
In recent years,the trifluoromethoxy(OCF3)functional group has received extensive attention in phar-maceuticals,agrochemicals and material sciences.However,the methods for the enantioselective syn-thesis of trifluorom...
关键词：methoxyl REAGENT CENTERS 
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