金珠果梨香气成分GC-MS分析研究  

Analysis of Jinzhuguo Pear Aroma Components by GC-MS

作　　者：马越[1] 谢国莉[1] 许肇初 韩玛莉娜 曹奇光[1] 陈红梅[1] MA Yue;XIE Guo-li;XU Zhao-chu;HAN Ma Li-na;CAO Qi-guang;CHEN Hong-mei(College of Bioengineering,Beijing Polytechnic,Beijing 100176,China;Food Institute Shenyang Agricultural University,Shenyang 110866,Liaoning,China)

机构地区：[1]北京电子科技职业学院生物工程学院,北京100176 [2]沈阳农业大学食品学院,辽宁沈阳110866

出　　处：《食品研究与开发》2018年第12期138-144,共7页Food Research and Development

基　　金：促进人才培养(学生综合素质培养)-生物工程学院学生科学研究能力提升项目(CJRC-XSZH-2015/004);北京电子科技职业学院科技重点课题(YZK2014022)

摘　　要：采用顶空固相微萃取(headspace solid phase microextraction,HS-SPME)和气相色谱与质谱联用技术(gas chromatography with mass spectrometry,GC-MS)分析金珠果梨中梨皮、梨肉、梨汁中的香气成分,结果表明:共鉴定出香气成分53种。梨皮、梨肉、梨汁样品中均含有大量正己酸乙酯、丁酸乙酯、辛酸乙酯,梨皮样、梨肉样及梨汁样中3种酯的总和分别占香气物质的69.42%、30.90%、29.15%。除此之外还含有己烯醛、壬醛、癸醛,且3种醛总含量分占梨皮样、梨肉样及梨汁样中香气物质的10.38%、12.88%、7.13%。这些香气成分可使金珠果梨具有怡人的风味,并使金珠果梨具有自身的典型性风格。此外,金珠果梨果皮香气成分比较丰富,共鉴定出30种,其中特有成分十余种,在加工果汁、果脯、罐头等产品时,尽量保留果皮,以保留产品独特香气。金珠果梨果汁中香气成分共鉴定出30种,其中独特成分15种,因此,适宜加工生产果汁产品。Headspace solid phase microextraction（HS-SPME）and gas chromatography-mass spectrometr y（GC-MS）were used in the present study to analyze the aroma components in Jinzhuguo pear,pear peal and pear juice. The results showed that the 53 kinds of aroma components were detected in total. Pear peel,pear and pear juice samples contain large amounts of positive ethyl hexanoate,ethyl butyrate,ethyl octanoate with the sum of these three esters accounting for 69.42 %,30.90 % and 29.15 %,respectivly. In addition,hexenal,nonanal and decanal were also detected with the total amount accounting for 10.38 %,12.88 % and 7.13 %,respectively,in pear,pear peal and pear juice. These fragrances make Jinzhuguo pear have a pleasant flavor and have its own typical style. 30 aroma components were identified in the peal of jinzhuguo pear,and about10 of them were unique. Thus,peal is recommended to be reserved in processing fruit juice,preserved fruit and canned products in order to keep the unique aroma. There were 30 kinds of aroma components in the fruit juice,and 15 of them were unique. Therefore,it is suitable for Jinzhuguo pear to be processed into fruit juice products.

关 键 词：气相色谱-质谱联用技术 金珠果梨 香气成分 定量定性分析 对比研究 

分 类 号：O657.63[理学—分析化学] TS255.7[理学—化学]