Supported by the National Natural Science Foimdation of China(No.31701827);the Natural Science Foundation of Shandong Province, China(Nos.ZR2017BH037,ZR2017BC053).
In order to develop a novel herbicide containing the 2,1-benzothiazine motif, a series of 3-acetyl-4- hydroxy-2,1-benzothiazine derivatives was synthesized. All the target compounds were confirmed by 1H NMR,13C NMR, a...
Supported by the National Natural Science Foundation of China(No.21376255).
To investigate the green trinitration method of aromatic compounds, with Lewis acid/ionic liquid as catalyst and HNOJAc2O as nitration reagent, a Lewis acid/ionic liquid/HNO3/Ac2O system was established. In various co...
Supported by the National Natural Science Foundation of China(No.29571013).
The lowest triplet energy levels of the six ligands(T) were determined to be 22989 cm-1[1,3-bis-(1'-phenyl-3'-methyl-5'-pyrazolon-4')-1,3-propanedione,BPMPTD],23148 cm-1[1,4-bis-(1'-phenyl-3'-methyl-5'-pyr...
A convenient and environmentally friendly reactor for the synthesis of glycosyl bromides via ultrasound irradiation was designed. Peracetylated glycosyl bromides were synthesized from free saccharides by means of a on...
Supported by the National Technology-Innovation Fund(No.02CJ-13-01-16);the Open Fund of State Key Laboratory of Pharmaceutical Biotechnology of Nanjing University, China
Lacosamide was prepared by chemical method coupled with enzymatic method. N-Acetyl-D, L-3-methoxy-alanine, derived from D,L-3-methoxy-alanine, was used in the resolution process catalyzed by immobilized Escherichia co...
Supported by the Key Laboratory of Rare Earth Functional Materials of Shanghai City,China(No.07dz22303);the Key Scientific and Technological Project of Shanghai City,China(No.09391912100)
2,4-Dichlorophenoxyacetyl(thio)urea and S-(+)-3-methyl-2-(4-chlorophenyl)butyramides were synthesized via acylation,aminolysis,esterification and addition reactions,and the partial new compounds have desirable ...
Supported by the Natural Science Foundation of Tianjin, China(No.07JCZDJC05400).
1 Introduction Centipeda minima(Compositae) is an annual herbaceous plant found in moist places throughout the plains mainly in the southern regions of the People's Republic of China, Eastern tropical Asia, Austra...
The crystal and molecular structures of O-ethyl-N-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-thiocarbamate were determined by X-ray crystallography. It crystallizes in the orthorhombic system with space group P2(1)2(1)2(...
the National Nature Science Foundation of China(No.30 17110)
A practical and scalable synthesis route of acetylphenylboronic acids is described. Bromoacetophenones(compounds 3a, 3b) were ketalized with ethylene glycol and triethyl orthoformate to give bromo ketals(compounds 4a_...