supported by the National Natural Science Foundation of China(Nos.21272154 and 81202402)。
Three C-3’-N-sulfonyl and C-7-O-acyl paclitaxel analogues were synthesized from 10-deacetyl baccatinⅢ(10-DAB)and their structures were confirmed by 1H NMR,13C NMR and HR-MS.Among them,the crystal structure of compou...
funded by the Public Science&Technology Project of Zhejiang Province(No.2017C32011);Mid-Youth Academic Team of Zhejiang Shuren University;Natural Science Foundation of Zhejiang Province(No.LY19C140002)
The title compound 3-(difluoromethyl)-1-methyl-N-((2-(trifluoromethyl)phenyl)-carbamoyl)-1 H-pyrazole-4-carboxamide(C14 H11 F5 N4 O2) was synthesized, and its structure was confirmed by 1 H NMR, H RMS and X-ra...
Financial support from the National Natural Science Foundation of China(No.81773746);the Open Project of Hubei Key Laboratory of Wudang Local Chinese Medicine Research,Hubei University of Medicine(No.WDCM009 and 2011JH-2014CXTT07);the Foundation of Health and Family planning Commission of Hubei Province(No.WJ2015Z113);the Foundation for Innovative Research Team of Hubei University of Medicine(2014CXZ01 and 2014CXZ05)
A series of 2-acyl-β-lactam-2-carboxamides was prepared through a tandem Ugi 4 CC/SN cyclization of bromoacetic acid, primary amine, arylglyoxal, and isocyanide. All of them were characterized by NMR, IR, MS and elem...
supported by the National Natural Science Foundation of China(31772208);Heilongjiang Province Postdoctoral Science Foundation(LBH-Z16033)
Two novel N-acyl-3-phenylpyrazol benzophenones were designed and synthesized via cyclization and acylation with 1,3-diphenylpropane-1,3-dione and dimethylformamide dimethylacetal as the starting materials.Both of the ...
supported by the National Natural Science Foundation of China(21273171);Natural Science Foundation of Shangluo University(16SKY005);Special Scientific Research Project of Education Department of Shaanxi Province Government(17JK0242)
2-Carbonyl propionic acid-4-methyl benzoyl hydrazone (PAMH) has been synthe-sized by using 4-methyl benzoyl hydrazine and pyruvic acid as the chemicals and acetic acid asphase transfer catalyst under microwave radia...
Supported by the National Science Foundation of China(No.21161019,21301146);Natural Science Fund for Distinguished Young Scholars of Xinjiang Uygur Autonomous(No.2013711008);Technological Innovation Youth Training Project of Xinjiang Autonomous(No.2013721017)
[Zn(L)(CH3OH)3](H2L = N-(1-phenyl-3-methyl-4-propenylidene-5-pyrazolone)-salicylidene hydrazide) has been synthesized by the reaction of zinc nitrate and ligand H2 L. The complex crystallizes in orthorhombic s...
supported by the National Basic Research Program of China(2010CB126100)
A new crystal of O,Oˊ-dipropyl-α-(2,4-dichlorolphenoxyacylamido)-α-(4-methoxyphenyl) methylphosphonates has been prepared at room temperature and characterized by elemental analysis and IR,MS,1H NMR spectra,13C...
Supported by the Natural Science Foundation of Anhui Province (090416234);the National Natural Science Foundation of China (20901002);the Doctoral Startup Foundation of Anhui Normal University
A novel adamantane acyl amide derivative containing two phthalimido pendant groups(C31H31N3O5) has been synthesized,and its structure was characterized by elemental analysis,IR,1 H NMR spectra,and single-crystal X-r...
Project supported by the National Science Foundation of China
The crystal and molecular structure of(u-C2H5S)[μ-CO-C(CH3)-CH2]Fe2(CO)6, Mr = 409.958 has been determined by X-ray diffraction method. Crystals of this complex are monoclinic, belonging to space group P21/c, and the...