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A general bottom-up synthesis of CuO-based trimetallic oxide mesocrystal superstructures for efficient catalytic production of trichlorosilane被引量：1: 《Nano Research》2020年第10期2819-2827,共9页Hezhi Liu Yongjun Ji Jing Li Yu Zhang Xueguang Wang Haijun Yu Dingsheng Wang Ziyi Zhong Lin Gu Guangwen Xu Yadong Li Fabing Su; the National Natural Science Foundation of China(Nos.21878301,21978299,and 21908224);Z.Z.thanks the kind support of Guangdong Technion Israel Institute of Technology(GTTIT)for the collaboration.; Mesocrystals, the non-classical crystals with highly ordered nanoparticle superstructures, have shown great potential in many applications because of their newly collective properties. However, there is still a lack o...; 关键词：CuO-based trimetallic oxide mesocrystal SUPERSTRUCTURES catalytic production of trichlorosilane synthesis strategy

Quartz Crystal Microbalances for Evaluating Gas Motion Differences between Dichlorosilane and Trichlorosilane in Ambient Hydrogen in a Slim Vertical Cold Wall Chemical Vapor Deposition Reactor被引量：1: 《Advances in Chemical Engineering and Science》2020年第3期190-200,共11页Mana Otani Toshinori Takahashi Hitoshi Habuka Yuuki Ishida Shin-Ichi Ikeda Shiro Hara; A dichlorosilane gas and a trichlorosilane gas in ambient hydrogen were evaluated to show their different gas flow motions in a slim vertical cold wall chemical vapor deposition reactor for the Minimal Fab system. Thi...; 关键词：Minimal Fab Chemical Vapor Deposition Reactor Quartz Crystal Microbalance Silicon Epitaxial Growth TRICHLOROSILANE DICHLOROSILANE

Application of Energy Saving Technology in Trichlorosilane Distillation Purification Process: 《China Petroleum Processing & Petrochemical Technology》2019年第3期94-102,共9页Qie Siyuan Pang Weiwei Zhao Ming Huang Zheqing; financial support from the National Natural Science Foundation of China (project No. 21406157); The trichlorosilane(TCS)purification process consumes a significant amount of energy to achieve the high purity requirement for TCS quality(99.9999%).This work proposed a series of energy saving technology to enhance ...; 关键词：TRICHLOROSILANE DISTILLATION PURIFICATION ENERGY SAVING technology PROCESS simulation

Experimental Study on Hydrogenation of SiCl_4 to SiHCl_3 in a Stirred Bed Reactor: 《过程工程学报》2016年第5期767-773,共7页李庆远李佩龙王铁峰; The hydrogenation of SiCl_4 to SiHCl_3 was studied in a stirred bed reactor with CuCl catalyst.The properties of the CuCl catalysts and silicon particles before and after the reaction were characterized by SEM,XRD and...; 关键词：silicon tetrachloride TRICHLOROSILANE HYDROGENATION stirred bed reactor

Carbohydrate-Derived Organocatalysts for the Reduction of Imines with Trichlorosilane: 《Journal of Materials Science and Chemical Engineering》2015年第6期48-53,共6页Xin Ge Chao Qian Xinzhi Chen; The backbone of D-glucosamine hydrochloride was fine-tuned and modified by protecting the hydroxyl groups. In order to reduce imines with trichlorosilane, the carbohydrate-derived organocatalysts were prepared and scr...; 关键词：CARBOHYDRATE ORGANOCATALYST REDUCTION Imine

Thermodynamic analysis of manufacturing polysilicon from Si HCl_3,Si Cl_4 and H_2被引量：1: 《Chinese Journal of Chemical Engineering》2015年第4期681-688,共8页李佩龙王铁峰; Supported by the Beijing New Star Project on Science & Technology of China(2009B35);the Program for New Century Excellent Talents in University(NCET-12-0297); Production of polysilicon by chemical vapor deposition of SiHCI3 with a fluidized bed reactor is a competitive technology. As equilibrium conversion can be approached in a fluidized bed reactor, a reliable thermodynam...; 关键词：ThermodynamicsPolysiliconFluidized bedTrichlorosilaneSilicon tetrachtoride

Simulation of Reactive Distillation Process for Monosilane Production via Redistribution of Trichlorosilane被引量：1: 《Chinese Journal of Chemical Engineering》2014年第3期287-293,共7页孙帅帅黄国强; The reactive distillation process for producing high purity monosilane via trichlorosilane redistribution reaction was simulated. Rigorous RadFrac block was employed in Aspen Plus simulation package. Accurate results ...; 关键词：reactive distillation reaction kinetics trichlorosilane redistribution pumparound monosilane

Recyclable Cyclohexanediamine Derivatives as Organocatalysts: Organocatalytic Reduction with Trichlorosilane and Aldol Reaction: 《International Journal of Organic Chemistry》2013年第4期240-242,共3页Yuya Tanimura Kaori Ishimaru; Reduction of ketimine with trichlorosilane was carried out using bisformamide catalyst 1a derived from cyclohexanediamine to give the corresponding product in 81% yield with 39% ee. Deprotection of the formyl groups o...; 关键词：Aldol Reaction Cyclohexanediamine ORGANOCATALYSIS RECYCLABLE REDUCTION

Asymmetric Synthesis of Novel Axially Chiral 2,2＇-Bipyridine N,N＇-Dioxides Bearing α-Amino Acid Residues and Their Applications in Enantioselective Allylation of Aromatic Aldehydes with Allyltrichlorosilane被引量：1: 《Chinese Journal of Chemistry》2013年第4期485-493,共9页Hongwu Zhao Yuanyuan Yue Hailong Li Zhihui Sheng Zhao Yang Wei Meng; We thank Beijing Municipal Commission of Edu- cation （No. JC015001200902）, Beijing Municipal Natu- ral Science Foundation （Nos. 710201, 2122008）, Basic Research Foundation of Beijing University of Technol- ogy （X40 15001201101）, Funding Project for Academic Human Resources Development in Institutions ofHigher Learning Under the Jurisdiction of Beijing Municipality （No. PHR201008025）, Doctoral Scientific Research Start-up Foundation of Beijing University of Technology （No. 52015001200701） for financial sup- ports.; A series of novel axially chiral 2,2＇-bipyridine N,N＇-dioxides bearing C1 or C2-symmetry have been synthesized by the use of enantiopure a-amino acids as chiral sources. The absolute stereochemistry of the axial chi...; 关键词：2 2＇-bipyridine N N＇-dioxide organocatalyst asymmetric catalysis enantioselective allylation allyl-trichlorosilane

Formation of Chiral a-Monofluorinated-.8-amino Esters through Organocatalytic Asymmetric Reduction of a-Fluoro-j3-enamino Esters by Trichlorosilane: 《Chinese Journal of Chemistry》2012年第11期2636-2640,共5页张鹏王超周莉孙健; Acknowledgement We are grateful for financial supports from the Na- tional Natural Science Foundation of China （Project Nos. 20972151, 21272227 and 91013006）.; A concise method was developed to prepare chiral a-monofluorinated-β-amino esters through N-sulfinyl urea catalyzed asymmetric hydrosilylation of a-fluoro-β-enamino esters, which affords high yields, good to high di...; 关键词：asymmetric reduction sulfinyl urea a-fluorinated-β-amino ester STEREOSELECTIVITY

TRICHLOROSILANE