CHIRAL_STATIONARY_PHASE

作品数：46被引量：49H指数：3
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相关作者：段蓉陈伟王昭君柏正武更多>>
相关机构：武汉工程大学更多>>
相关期刊：《Chemical Research in Chinese Universities》《Journal of Zhejiang University-Science B(Biomedicine & Biotechnology)》《Chinese Journal of Chemistry》《Chinese Journal of Chemical Engineering》更多>>
相关基金：国家自然科学基金湖北省自然科学基金更多>>
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Synthesis of Proline-Derived Helical Copolyacetylenes as Chiral Stationary Phases for HPLC Enantioseparation
《Chinese Journal of Polymer Science》2025年第1期61-69,I0007,共10页Yue Li Shu-Ming Kang Ge Shi Yi-Fu Chen Bo-Wen Li Jie Zhang Xin-Hua Wan 
supported by the National Natural Science Foundation of China(Nos.52273002 and 52333008);the funding of Boya Postdoctoral Fellowship at Peking University,BMS Junior Fellow Program and the National Funding Program for Postdoctoral Researchers(No.GZC20230031).
A series of optically active copolymers with various feed ratios have been synthesized through helix-sense-selective copolymerization catalyzed by[Rh(norbornadiene)Cl]2-triethylamine.This process involves two proline-...
关键词：Helical copolyacetylene Chiral stationary phase High performance liquid chromatography ENANTIOSEPARATION Hydrogen bonding 
Chiral Method Development Using Polysaccharide-Based Chiral Stationary Phase (CSP) and Investigation of Chiral Column Degradation and Regeneration
《American Journal of Analytical Chemistry》2024年第12期395-406,共12页Hua Zhao Mary Ababat Kyle Leeman John Tucker 
Two polysaccharide-based chiral stationary phase columns were evaluated to improve the previous partial chiral peak separation to a baseline-resolved separation of the INGREZZA® drug substance and its diastereomers. M...
关键词：Chiral Reversed-Phase HPLC Separation Backflush Chiral Column Regeneration INGREZZA® (Valbenazine) 
A chiral metal-organic framework{(HQA)(ZnCl_(2))(2.5H_(2)O)}n for the enantioseparation of chiral amino acids and drugs
《Journal of Pharmaceutical Analysis》2023年第4期421-429,共9页Xiangtai Zheng Qi Zhang Qianjie Ma Xinyu Li Liang Zhao Xiaodong Sun 
This study was funded by the National Natural Science Foundation of China(Grant No.:82003705);the Shanghai Science and Technology Innovation Foundation(Grant Nos.:23010500200 and 23ZR1422700).
Chiral metal-organic frameworks(CMOFs)with enantiomeric subunits have been employed in chiral chemistry.In this study,a CMOF formed from 6-methoxyl-(8S,9R)-cinchonan-9-ol-3-carboxylic acid(HQA)and ZnCl_(2),{(HQA)(ZnCl...
关键词：Capillary electrochromatography Metal-organic framework ENANTIOSEPARATION Chiral stationary phase Open-tubular column Dansyl amino acids 
MIL-53-based homochiral metal-organic framework as a stationary phase for open-tubular capillary electrochromatography被引量：2
《Journal of Pharmaceutical Analysis》2022年第3期509-516,共8页Xiaodong Sun Bing Niu Qi Zhang Qin Chen 
funded by the National Natural Science Foundation of China(Grant No.:82003705).
Homochiral metal-organic frameworks(MOFs)have attracted considerable attention in many fields of research,such as chiral catalysis and chiral chromatography.However,only few homochiral MOFs can be effectively used in ...
关键词：Homochiral MOF L-His-NH-MIL-53 Chiral stationary phase Capillary electrochromatography ENANTIOSEPARATION 
A β-cyclodextrin covalent organic framework used as a chiral stationary phase for chiral separation in gas chromatography被引量：1
《Chinese Chemical Letters》2022年第2期898-902,共5页Bo Tang Wei Wang Huipeng Hou Yiquan Liu Zongkun Liu Lina Geng Liquan Sun Aiqin Luo 
financially supported by the National Key R&D Program of China (No.2019YFA0904104)。
Chiral covalent organic frameworks(CCOFs) featuring chirality, stability, and good porosity have attracted a considerable amount of attention due to their important applications, such as asymmetric catalysis, chiral s...
关键词：Β-CYCLODEXTRIN Covalent organic framework Chiral stationary phase Gas chromatography ENANTIOSEPARATION 
Preparation and chromatographic evaluation of a chiral stationary phase based on carboxymethyl-β-cyclodextrin for high-performance liquid chromatography被引量：1
《Chinese Chemical Letters》2018年第9期1399-1403,共5页Min Zhou Yuande Long Yonggang Zhi Xiaoying Xu 
A chiral stationary phase （CSP） was prepared by chemically bonding carboxymethyl-β-cyclodextrin （CM- β-CD） onto 3-aminopropyl silica gel through amidation reaction in water solution and was characterized by Four...
关键词：ENANTIOSEPARATION Carboxymethyl-β-cyclodextrin Chiral stationary phase Chemical bonding REVERSED-PHASE 
Unusual retention behavior of omeprazole and its chiral impurities B and E on the amylose tris(3-chloro-5-methylphenylcarbamate)chiral stationary phase in polar organic mode被引量：2
《Journal of Pharmaceutical Analysis》2018年第4期234-239,共6页Rosella Ferretti Leo Zanitti Adriano Casulli Roberto Cirilli 
funding from the European Community's Seventh Framework Programme under the grant agreement 602051 (Project HERACLES: Humancystic Echinococcosis Rese Arch in Centra L and Eastern Societies; http://www.Heracles-fp7.eu/)
Recent reports have demonstrated that the new commercially available immobilized-type chiral stationary phases（CSPs） containing amylose tris（3-chloro-5-methylphenylcarbamate）（ACMPC） as a selector exhibit not onl...
关键词：Chiralpak IG-3 Retention Enantioselective HPLC OMEPRAZOLE Column temperature Basic/acid additives 
A New and Enantioselective Chromatographic Method for Linagliptin on Amylose Coated Chiral Stationary Phase
《American Journal of Analytical Chemistry》2016年第7期556-567,共12页Cholleti Vijay Kumar Pasula Aparna Pavan Kumar Vasa Y. Ravindra Kumar Nitin Haridas Dhekale 
A new and enantioselective liquid chromatographic method was developed for estimation of S-Linagliptin in Linagliptin (LINA) drug substances. The desired enantiomeric separation was achieved on Chiralpak AD-H (250*4.6...
关键词：ENANTIOMERS Amylose Based Stationary Phase Method Development Method Validation SPECIFICITY 
Preparation and chromatographic characteristics of a novel 2,6-dimethyl-β-CD bonded HPLC chiral stationary phase被引量：1
《Chinese Chemical Letters》2014年第11期1416-1418,共3页Qiu-Jin Peng Jun-Jiao Yang 
A novel 2,6-dimethyl-b-CD bonded and silica based HPLC chiral stationary phase（CSP） was prepared.The diphenylmethane diisocyanate（MDI） was applied for the first time in the immobilization of 2,6-dimethyl-b-CD onto...
关键词：2 6-Dimethyl-b-cyclodextrin Chiral stationary phase（CSP） Diphenylmethane diisocyanate（MDI） Chiral separation 
Preparation and Enantioseparation Property of Chiral Stationary Phases Based on Cellulose Tris(3,5-dimethylbenzoate)——A New Way to Prepare Polysaccharide-coating Type Chiral Stationary Phases被引量：1
《Chinese Journal of Polymer Science》2014年第4期458-466,共9页Wei Chen Rong Duan Qing-chun Fan 柏正武 黄少华 
financially supported by the National Natural Science Foundation of China(No.50973086);Hubei Provincial Department of Education of China(Z 20081501)
A new method to prepare polysaccharide-coating type chiral stationary phases （CSPs） was developed in this work. As a typical example, naked silica gel was coated by cellulose, which was then derivatized with 3,5-dim...
关键词：Cellulose tris（3 5-dimethylbenzoate） Chiral recognition Chiral stationary phase High-performance liquidchromatography. 
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