CHROMATOGRAPHIC

作品数:124被引量:225H指数:7
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Chiral metal-organic frameworks-based materials for chromatographic enantioseparation
《Chinese Chemical Letters》2024年第12期111-124,共14页Genlin Sun Yachun Luo Zhihong Yan Hongdeng Qiu Weiyang Tang 
supported by the Science and Technology Project of Education Department of Jiangxi Province (No.GJJ201249)。
The homochiral compounds play an important role in human health and pharmaceutical industry.Currently,the chromatographic enantioseparation has become one of the most effective and practical approach to obtain pure en...
关键词:CHIRALITY Racemic separation Chiral metal-organic frameworks Chromatographic technology Chiral stationary phases 
Preparation and chromatographic evaluation of a chiral stationary phase based on carboxymethyl-β-cyclodextrin for high-performance liquid chromatography被引量:1
《Chinese Chemical Letters》2018年第9期1399-1403,共5页Min Zhou Yuande Long Yonggang Zhi Xiaoying Xu 
A chiral stationary phase (CSP) was prepared by chemically bonding carboxymethyl-β-cyclodextrin (CM- β-CD) onto 3-aminopropyl silica gel through amidation reaction in water solution and was characterized by Four...
关键词:ENANTIOSEPARATION Carboxymethyl-β-cyclodextrin Chiral stationary phase Chemical bonding REVERSED-PHASE 
Studies of the intestinal absorption of the alkaloids in the Wu-tou decoction combined with different incompatible medicinal herbs in a Caco-2 cell culture system using UPLC-MS/MS被引量:5
《Chinese Chemical Letters》2015年第5期590-594,共5页Hong Kan Wen-Yue Jiang Ru Ding Zhong-Ying Liu Zi-Feng Pi Zhi-Qiang Liu 
supported by the National Natural Sciences Foundation of China(No.81274046);National Basic Research Program of China("973 Program")(Nos.2011CB505300, 2011CB505305)
In this study, seven alkaloids were detected in Wu-tou decoction using ultra performance liquid chromatography coupled with tandem mass spectrometry (UPLC-MSn). The aim of this study was to investigate the effect of...
关键词:Wu-tou decoction Caco-2 cell Ultra performance liquid chromatographic coupled with tandem mass spectrometry (UPLC-MS/MS~) incompatible herbs 
Preparation and chromatographic characteristics of a novel 2,6-dimethyl-β-CD bonded HPLC chiral stationary phase被引量:1
《Chinese Chemical Letters》2014年第11期1416-1418,共3页Qiu-Jin Peng Jun-Jiao Yang 
A novel 2,6-dimethyl-b-CD bonded and silica based HPLC chiral stationary phase(CSP) was prepared.The diphenylmethane diisocyanate(MDI) was applied for the first time in the immobilization of 2,6-dimethyl-b-CD onto...
关键词:2 6-Dimethyl-b-cyclodextrin Chiral stationary phase(CSP) Diphenylmethane diisocyanate(MDI) Chiral separation 
Optimization by orthogonal array design of ion-pair HPLC separation of the enzymatic hydrolysis products of yeast RNA被引量:3
《Chinese Chemical Letters》2010年第12期1453-1456,共4页Jie Hua Ke Long Huang 
The separation of enzymatic hydrolysis products of yeast RNA by ion-pair HPLC was studied.A modified chromatographic response function(MCRF) was proposed to appraise the effectiveness of chromatographic separation.T...
关键词:Chromatographic response function Orthogonal array design 5'-Phosphodiesterase Barley roots NUCLEOTIDES 
Synthesis and Chromatographic Properties of New β-Cyclodextrin Derivatives with α-Schiff Base Groups for HPLC
《Chinese Chemical Letters》2005年第6期789-792,共4页MinFANG ZhiMingZHOU AiQinLUO 
Cyclodextrin 1 was directly oxidized to the corresponding monoaldehyde 2 on their primary faces by cyclized 2-iodoxybenzoic acid(IBX) in DMSO, followed by the synthesis of β-cyclodextrin derivatives bearing Schiff-ba...
关键词:CYCLODEXTRIN Schiff base ferrocene. 
A Highly Sensitive Kinetic Spectrophotometric System and Its Analytical Potential for Chromatographic Detection of Metal Ions
《Chinese Chemical Letters》1999年第1期51-54,共4页Xi Rong HUANG Wen Juan ZHANG Shu Hua HAN Gut Ying XU(College of Chemistry, Shandong University, Jinan 250100) 
Based on the inhibitory effect of metal ions on the decolourization reaction of a dye taking place in a mixed micellar medium, a differential rate method was developed for the detection of metal ions. The present kine...
关键词:mixed micellar media decolourization reaction bromopyrogallol red metal ions INHIBITOR SPECTROPHOTOMETRY method development 
High-Performance Liquid Chromatographic Determination Of N-Nitrosoamines by Pre-Column Fluorescence Derivatization with 9-Phenanthrene Chloride
《Chinese Chemical Letters》1996年第12期1113-1116,共4页JinMao YOU Bin ZRAO QingCun ZHU(Department of Chemistry, Qufu Normal University, Qufu. Shandong 273 165) 
A sensitive high-performance chromatographic method for the detection of N-nitrosoamines with pre-column fluorescence derivatization has been developed.Eight representative N-nitrosoamines, which were separated on a r...
关键词:Pre Nitrosoamines COLUMN DERIVATIZATION CHLORIDE 
Reversed-Phase High-Performance Liquid  Chromatographic Determination of Drugs of Abuse
《Chinese Chemical Letters》1996年第11期1027-1028,共2页Ma, C Duan, HJ Xu, YQ Zhou, TH 
A high-performance liquid chromatographic method using uv detection for thedetermination of 10 drugs of abuse is described. The method is sample and sensitive. The linear rangesare 20 ̄100ng/ml with relative standard ...
关键词:DETERMINATION DRUGS ABUSE CHROMATOGRAPHIC 
MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHIC SEPPATION OF PYRIMIDINE AND PURINE DERIVATIVES
《Chinese Chemical Letters》1996年第4期347-350,共4页Zhou Bin YUAN yong CHEN Ping REN Feng Mei HAN(The Graduate School,USTC.Academia Sinica, beijing 100039) 
The retention behaviours of 12 purine and pyrimidine derivatives thymine,uracil,cytosine,adenine,guanine,xanthine,hypoxanthine, purine, 4,6 diaminopyrimidine,tpeophylline,trimethoprimum and 6 (benzylamino)purine...
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